"Carbamothioates in the synthesis of diaroyl sulfides; selectivity in t" by Ashraf A. Aly, Alan B. Brown et al.
 

Document Type

Article

Publication Title

Arkivoc

Abstract

Diaroyl sulfides were prepared in one-pot reaction from ethylenediamine and carbon disulfide, via reaction of in situ generated ethylene-bis- carbamodithioates with aroyl chlorides. The reaction of diaroyl sulfides with acetylenic and ethylenic π-deficient compounds such as dimethyl acetylenedicarboxylate, ethyl propiolate, (E)-1,4-diphenylbut-2-ene-1,4-dione and 1,4-diphenylbut-2-yne-1,4-dione afforded the corresponding thionylated products. NMR spectroscopic data of the isolated products were discussed. © ARKAT USA, Inc.

First Page

66

Last Page

77

DOI

10.3998/ark.5550190.0010.d06

Publication Date

12-4-2009

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